EXTRACTION AND OPTIMIZATION OF DYEING CONDITIONS OF DYE OBTAINED FROM PURPLE SWEET POTATO ON COTTON FABRICS

Authors

  • SAMSON ANA Department of Industrial Chemstry, Federal University, Wukari, Nigeria
  • SAMSON PAUL Department of Pure and Applied Chemistry, University of Calabar, Nigeria
  • AHMAD FALALU LADAN Department of Chemistry Federal University of Technology AkureOndo State
  • GBENGA EMMANUEL ADEKAYERO Department of Chemistry Federal University of Technology AkureOndo State
  • MUSA YAHAYA ABUBAKAR Department of Industrial Chemstry, Federal University, Wukari, Nigeria

DOI:

https://doi.org/10.22159/ijcr.2026v10i1.316

Keywords:

Purole sweet potato, Natural dye, Anthocxyanin and optimized dyed fabric

Abstract

Objective: This study aimed to isolate anthocyanidins from purple sweet potato (Ipomoea batatas) and to determine the optimum dyeing conditions for achieving maximum color yield and fabric affinity when dyeing cotton fabrics, as a sustainable alternative to synthetic dyes.

Methods: Anthocyanidins were extracted from purple sweet potato using acidified ethanol to ensure pigment stability. Dyeing parameters including temperature (40–80 °C), pH (3–9), and dyeing time (30–90 min) were systematically optimized. UV–Vis spectroscopy was employed to identify anthocyanidins based on characteristic absorption peaks at 520–540 nm, while FTIR analysis was used to confirm the presence of functional groups associated with anthocyanidins and to assess structural integrity after extraction.

Results: The UV–Vis spectra confirmed the presence of anthocyanidins through characteristic absorption peaks, while FTIR analysis revealed functional groups such as hydroxyl and aromatic rings, indicating that the extracted pigments remained structurally intact. Optimal dye uptake was achieved at a dyeing temperature of 80 °C and pH 3. Longer dyeing times (90 min) resulted in more uniform coloration on cotton fabrics.

Conclusion: The results demonstrate that anthocyanidins extracted from purple sweet potato are effective natural dyes for cotton fabrics. Under optimized dyeing conditions, these pigments exhibit good color uptake and uniformity, indicating their strong potential as environmentally friendly and sustainable alternatives to synthetic dyes.

Downloads

Download data is not yet available.

References

1. Khan M. Rehman MSU, Khan A. Environmental implications of synthetic dyes in textile wastewater and sustainable alternatives. J Environ Manag. 2022;317:115353. doi: 10.1016/j.jenvman.2022.115353.

2. Li X, Huang Y, Lu Y, Jia T, Wang J, Li P. N-doped GO cathode catalyst boosting capacity of denitrification for air-cathode microbial fuel cell by shifting microbial community composition in treating marine wastewater. J Water Process Eng. 2023;53:103687. doi: 10.1016/j.jwpe.2023.103687.

3. Saxena S, Raja AS. Eco-sustainability in textile coloration using natural dyes: challenges and future prospects. Sustain Chem Pharm. 2022;25:100569. doi: 10.1016/j.scp.2021.100569.

4. Rani R, Sharma D, Kaur P. Natural dyes as sustainable alternatives: current trends and future perspectives. Mater Today Proc. 2021;47:4021-7. doi: 10.1016/j.matpr.2021.04.281.

5. Yabalak E, Erdogan Eliuz EA. Green synthesis of walnut shell hydrochar its antimicrobial activity and mechanism on some pathogens as a natural sanitizer. Food Chem. 2022;366:130608. doi: 10.1016/j.foodchem.2021.130608, PMID 34454799.

6. Luo Z, Fang J, Wang X. Functional properties of anthocyanins from Ipomoea batatas: antioxidant activity and sustainable applications in textiles. Dyes Pigments. 2023;211:111030. doi: 10.1016/j.dyepig.2023.111030.

7. Zhang Y, Xu H, Huang Q. Ultrasound-assisted extraction of anthocyanins from purple sweet potato and their stability in textile dyeing. Ultrason Sonochem. 2021;70:105323. doi: 10.1016/j.ultsonch.2020.105323.

8. Abubakar MY, Garba F, Muhamad MA, Bioltif YE, Adam AB, Lawal U. Optimization of dyeing conditions of natural dye obtained from Vaccinium corymbosum (blueberry) on cotton fabric. Orbital: Electron J Chem. 2024;16(4):253–7. doi: 10.17807/orbital.v16i4.20223.

9. Ding Q, Jing L, Han W, Guan Y, Jiang Y, Wu C. Understanding the evolution of cellulose fibers during enzyme treatment. Ind Crops Prod. 2021;171:113983. doi: 10.1016/j.indcrop.2021.113983.

10. Kumari P, Singh R, Bhattacharya S. Plasma and enzymatic pretreatments to enhance natural dye uptake in cotton textiles. Cellulose. 2024;31(2):1121-37. doi: 10.1007/s10570-023-05345-9.

11. Arunkumar K, Kumar R, Shanmugam V. Nano-encapsulation of anthocyanin-based natural dyes for improved stability and textile applications. J Clean Prod. 2022;343:130964. doi: 10.1016/j.jclepro.2022.130964.

12. Castaneda Ovando A, Pacheco Hernandez ML, Paez Hernandez ME, Rodriguez JA, Galan Vidal CA. Chemical studies of anthocyanins: a review. Food Chem. 2009;113(4):859-71. doi: 10.1016/j.foodchem.2008.09.001.

13. Khoo HE, Azlan A, Tang ST, Lim SM. Anthocyanidins and anthocyanins: colored pigments as food pharmaceutical ingredients and the potential health benefits. Food Nutr Res. 2017;61(1):1361779. doi: 10.1080/16546628.2017.1361779, PMID 28970777.

14. Patras A, Brunton NP, O Donnell C, Tiwari BK. Effect of thermal processing on anthocyanin stability in foods; mechanisms and kinetics of degradation. Trends Food Sci Technol. 2010;21(1):3-11. doi: 10.1016/j.tifs.2009.07.004.

15. Zahid M, Bhatti IA, Malik SA. Eco-friendly dyeing of natural fibers using plant-based anthocyanins: optimization and fastness evaluation. J Clean Prod. 2022;356:131847. doi: 10.1016/j.jclepro.2022.131847.

16. Chang SK, Alasalvar C, Shahidi F. Review of dried fruits: phytochemicals, antioxidant efficacies and health benefits. J Funct Foods. 2016;21:113-32. doi: 10.1016/j.jff.2015.11.034.

17. Zhu S, Yu J, Liu S, Ding Y, Wang W, Zhou X. A bottom-up evaluation on cryoprotective potentials of gelatine from fish scale. Food Hydrocoll. 2022;124:107243. doi: 10.1016/j.foodhyd.2021.107243.

18. Luo C, Zhang H, Hou T. Characterization and stability of anthocyanins from purple sweet potato. Food Chem. 2021;352:129349. doi: 10.1016/j.foodchem.2021.12934.

19. Andrade JK, Barros RG, Pereira UC, Gualberto NC, De Oliveira CS, Shanmugam S. α-amylase inhibition, cytotoxicity and influence of the in vitro gastrointestinal digestion on the bioaccessibility of phenolic compounds in the peel and seed of Theobroma grandiflorum. Food Chem. 2022;373(B):131494. doi: 10.1016/j.foodchem.2021.131494, PMID 34753077.

20. Wang S, Li X, Xu Y, Yang Q. Ultrasound-assisted extraction and characterization of anthocyanins from purple sweet potato: optimization, stability and antioxidant properties. LWT Food Sci Technol. 2023;175:114612.

21. Ayele TB, Kim H, Lee Y, Park J. Extraction efficiency and stability of anthocyanins from purple-fleshed sweet potato under acidified solvent systems. Front Plant Sci. 2024;15:1426589. doi: 10.3389/fpls.2024.1426589.

22. Li R, Zhou Y, Liu X. Comparative analysis of anthocyanin content in purple sweet potato extracts using the pH differential and HPLC methods. Food Anal Methods. 2024;17(5):2134-46. doi: 10.1007/s12161-024-02863-3.

23. Kim YJ, Lee S, Park S. Structural characterization and FTIR analysis of anthocyanin extracts from purple sweet potatoes. Spectrochim Acta A Mol Biomol Spectrosc. 2023;302:122957. doi: 10.1016/j.saa.2023.122957.

24. Adeel S, Rehman F, Zuber M. Green pre-treatment and dyeing of cotton fabric with natural plant-based colorants: optimization through response surface methodology. J Nat Fibers. 2023;20(12):22311-25. doi: 10.1080/15440478.2023.2211341.

25. Ahmed A, Bhatti IA, Adeel S, Habib N. Optimization of dyeing conditions of cotton fabric using natural anthocyanin dyes extracted from plant sources. Text Res J. 2023;93(11):2185-97. doi: 10.1177/00405175231145608.

26. Hasan M, Rahman MT, Nasir M. Sustainable dyeing of cotton fibers using anthocyanin-rich plant extracts: process optimization and color fastness evaluation. Dyes Pigments. 2024;226:111697. doi: 10.1016/j.dyepig.2024.111697.

27. Lewis DM, Hawkes JA. Novel bleach activator compounds derived from the reaction of isocyanic acid with selected nucleophiles. Color Technol. 2022;139(4):355-68. doi: 10.1111/cote.12662.

28. International Organization for Standardization. ISO 105-B02:2014. Textiles-tests for colour fastness part B02: colour fastness to artificial light: Xenon arc fading lamp test. Geneva: ISO; 2014.

29. Zhou M, Liu D, Chen X. Color fastness and pH stability of anthocyanin-based natural dyes applied to cotton and silk fabrics. Front Mater Sci. 2023;10:1145123. doi: 10.3389/fmats.2023.1145123.

30. Bovell Benjamin AC. Sweet potato: a review of its past present and future role in human nutrition. Adv Food Nutr Res. 2007;52:1-59. doi: 10.1016/S1043-4526(06)52001-7, PMID 17425943.

Published

01-01-2026

How to Cite

ANA, SAMSON, et al. “EXTRACTION AND OPTIMIZATION OF DYEING CONDITIONS OF DYE OBTAINED FROM PURPLE SWEET POTATO ON COTTON FABRICS”. International Journal of Chemistry Research, vol. 10, no. 1, Jan. 2026, pp. 49-54, doi:10.22159/ijcr.2026v10i1.316.

Issue

Section

Research Article
Share |